| 发明名称 |
METHOD FOR JOINT PREPARATION OF MONO(CYCLOALKYL)DIMAGNESIUMBROMIDEFULLERENES(60) AND BIS(CYCLOALKYL)TETRAMAGNESIUMBROMID- EFULLERENES(60) |
| 摘要 |
FIELD: organic synthesis. SUBSTANCE: toluene solution of fullerene(60) interacts with excess of ether solution of alpha,sigma- dimagnesium bromide in presence of zirconacene dichloride as catalyst for 10-20 hr under argon atmosphere and normal conditions to give products with yields 62-88%. EFFECT: extended synthetic possibilities. 1 tbl, 8 ex
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| 申请公布号 |
RU2136688(C1) |
申请公布日期 |
1999.09.10 |
| 申请号 |
RU19980108113 |
申请日期 |
1998.04.29 |
| 申请人 |
INSTITUT NEFTEKHIMII I KATALIZA AN RESPUBLIKI BASH;INST NEFTEKHIMII I KATALIZA AN |
发明人 |
DZHEMILEV U.M.;NEFEDOV O.M.;IBRAGIMOV A.G.;TOMILOV JU.V.;KHAFIZOVA L.O.;DEEVA E.A.;USHAKOVA Z.I. |
| 分类号 |
C07F3/02;C01B31/02;(IPC1-7):C07F3/02 |
主分类号 |
C07F3/02 |
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