发明名称 Resolution of d,1-menthol
摘要 1-Menthol can be readily obtained from racemic menthol by conversion of the latter to the diastereomeric esters of an optically active amino acid and chromatographing the diastereomers. The separation of the diastereomeric esters is relatively insensitive to the support or to the solvent used as eluant, and satisfactory separation occurs under a broad variety of conditions. 1-Menthol can be obtained by base catalyzed hydrolysis of the purified diastereomer with high optical purity.
申请公布号 US4418225(A) 申请公布日期 1983.11.29
申请号 US19820338443 申请日期 1982.01.08
申请人 UOP INC. 发明人 HOUSE, DAVID W.
分类号 C07C29/09;C07C35/12;(IPC1-7):C07C35/12 主分类号 C07C29/09
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