摘要 |
1,243,292. Acrylonitrile copolymer filaments. JAPAN EXLAN CO. Ltd. 11 Sept., 1969 [13 Sept., 1968], No. 44995/69. Heading B5B. [Also in Division C3] An aqueous sodium thiocyanate solution of a copolymer of acrylonitrile, vinylidene chloride and methyl acrylate containing at least 70% by weight of acrylonitrile and as stabilizer a combination of sodium metabisulphite with dibutyl tin diacetate or tri-n-butyl phosphite is extruded into a sodium thiocyanate, coagulating bath. The resulting filaments are washed with water, stretched in boiling water to 10 times their initial length and wet-heat relaxed at 122‹ to 125‹ C. |