发明名称 COLOR STABLE RED-EMITTING PHOSPHORS
摘要 A process for preparing a Mn+4 doped phosphor of formula I;Ax[MFy]:Mn+4   I;includes gradually adding a first solution to a second solution gradually discharging the product liquor from the reactor while volume of the product liquor in the reactor remains constant; wherein A is Li, Na, K, Rb, Cs, or a combination thereof;M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Y, La, Nb, Ta, Bi, Gd, or a combination thereof;x is the absolute value of the charge of the [MFy] ion;y is 5, 6 or 7.;The first solution includes a source of M and HF and the second solution includes a source of Mn to a reactor in the presence of a source of A.
申请公布号 US2016244663(A1) 申请公布日期 2016.08.25
申请号 US201514950679 申请日期 2015.11.24
申请人 GENERAL ELECTRIC COMPANY 发明人 Murphy James Edward;Sista Srinivas Prasad
分类号 C09K11/61 主分类号 C09K11/61
代理机构 代理人
主权项 1. A process for preparing a Mn+4 doped phosphor of formula I Ax[MFy]:Mn+4   I the process comprising gradually adding a first solution comprising a source of M and HF and a second solution comprising a source of Mn to a reactor in the presence of a source of A, to form a product liquor comprising the Mn+4 doped phosphor; and gradually discharging the product liquor from the reactor while volume of the product liquor in the reactor remains constant;wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
地址 Schenectady NY US