发明名称 METHOD OF PRODUCING N,N-DIMETHYL-3-PHENYL-2-PROPYNE-1-AMINE
摘要 FIELD: chemistry. ^ SUBSTANCE: proposed invention pertains to organic chemistry, more specifically to the method of producing N,N-dimethyl-3-phenyl-2-propyne-1-amine. The method involves reacting phenylacetylene with excess bisamine in the presence of a vanadyl acetylacetonate catalyst (VO(acac)2) in an argon atmosphere at 85°C temperature and atmospheric pressure for a period of 4-8 hours. N,N-dimethyl-3-phenyl-2-propyne-1-amine output is 84-98%. ^ EFFECT: invention can be used in thin organic synthesis, particularly for making not easily accessible polycyclic compounds, as well as in synthesis of biologically active substances. ^ 1 tbl, 1 ex
申请公布号 RU2349579(C1) 申请公布日期 2009.03.20
申请号 RU20070126036 申请日期 2007.07.09
申请人 INSTITUT NEFTEKHIMII I KATALIZA RAN 发明人 DZHEMILEV USEIN MEMETOVICH;SHAJBAKOVA MARIJA GENNAD'EVNA;TITOVA IRINA GENNAD'EVNA;IBRAGIMOV ASKHAT GABDRAKHMANOVICH
分类号 C07C209/60;C07C211/28 主分类号 C07C209/60
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