发明名称 Purification of thermally unstable mater- - ials eg caprolactam
摘要 The crude product is rectified so that the major part of the product together with low boiling components is taken off as vapour overhead and the remainder of the product together with the higher boiling components is removed as liquid from the column sump. The vapour is then rectified so that the pure product is recovered as liquid from the sump and the low boiling components are removed as vapour overhead. The remainder of the product and heavy ends are also further rectified from which pure product is recovered as overhead and the heavy ends withdrawn from the sump are evaporated to recover the small amount of product, they still contain.
申请公布号 DE2035859(A1) 申请公布日期 1971.03.11
申请号 DE19702035859 申请日期 1970.07.18
申请人 发明人
分类号 C07D201/16 主分类号 C07D201/16
代理机构 代理人
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