发明名称 |
PRODUCTION OF BINUCLEAR DIMETHYLOL COMPOUND OF P-CRESOL |
摘要 |
PROBLEM TO BE SOLVED: To easily obtain 2,2'-methylenebis(6-hydroxy-4-methylphenol) useful as a starting raw material for a condensation reaction in high purity and yield by reacting p-cresol with formaldehyde in the presence of a basic catalyst and water at a specific temperature. SOLUTION: The objective compound of the formula can be produced by reacting (A) p-cresol with (B) formaldehyde at a molar ratio (A:B) of 1:(1-5) at 40-80 deg.C in the presence of (C) 0.1-2 times mol (based on the component A) of a basic catalyst (e.g. an alkali metal hydroxide) and (D) 4-20 times weight (based on the component C) of water. The reaction is preferably carried out by adding an aqueous solution of the component B to a system containing the components A, C and D. |
申请公布号 |
JPH09110765(A) |
申请公布日期 |
1997.04.28 |
申请号 |
JP19950270302 |
申请日期 |
1995.10.18 |
申请人 |
SUMITOMO CHEM CO LTD |
发明人 |
ICHIKAWA KOJI;KAMABUCHI AKIRA;OZAKI HARUKI |
分类号 |
B01J23/04;C07B61/00;C07C37/20;C07C39/12;C07C39/16 |
主分类号 |
B01J23/04 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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