发明名称 |
METHOD FOR PRODUCING DIANHYDROHEXITOL-BIS-(4- ACRYLOYLOXY)ACYLATE |
摘要 |
PROBLEM TO BE SOLVED: To provide a method for producing dianhydrohexitol-bis-(4-acryloyloxy) acylate represented by general formula 2. SOLUTION: In a first process, dianhydrohexitol bisacylate represented by general formula 3 is biacylated using a 3-halopropionyl halide, yielding the corresponding dianhydrohexitol-bis-[3-halopropionyloxy]arylate and in a second process, two hydrogen halide molecules are cleaved from the dianhydrohexitol- bis-[3-halopropionyloxy]arylate with the aid of a base. Consequently, high-purity dianhydrohexitol-bis-(4-acryloyloxy)acylate represented by general formula 2 is inexpensively obtained by an industrially simple method in a high yield.
|
申请公布号 |
JP2002155085(A) |
申请公布日期 |
2002.05.28 |
申请号 |
JP20010209856 |
申请日期 |
2001.07.10 |
申请人 |
CONSORTIUM ELEKTROCHEM IND GMBH |
发明人 |
BRADER LEONHARD;HAEBERLE NORMAN;KRIEGBAUM MARKUS |
分类号 |
C07D493/04;(IPC1-7):C07D493/04 |
主分类号 |
C07D493/04 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|