发明名称 |
PROCEDE DE PREPARATION DE SELS PRATIQUEMENT PURS D'OXYACIDES DEPHOSPHORE DE METEAUX DU GROUPE IV B DU TABLEAU PERIODIQUE |
摘要 |
<p>A process for the preparation of substantially pure phosphorus oxyacid salts of metals which comprises (a) reacting a compound of a metal of Group IV b containing metallic impurities with a phosphorus oxyacid or its reactive derivative in the presence of water; (b) separating the forming gelatinous precipitate of the phosphorus oxyacid salt of the metal of Group IV b from the mother liquor by filtration; (c) (i) converting the obtained filter cake to a fluid sol by means of shear agitation and then scattering the sol into a heating atmosphere to form a granular gel or (ii) drying the obtained filter cake, then pelletizing the dried cake to form a granular gel; and (d) extracting the granular gel of the phosphorus oxyacid salt of the metal of Group IV b with an acid or its vapor in the presence of water to thereby remove metallic impurities therefrom.</p> |
申请公布号 |
BE747563(A1) |
申请公布日期 |
1970.08.31 |
申请号 |
BED747563 |
申请日期 |
1970.03.18 |
申请人 |
MIZUSAWA KAGAKU KOGYO K.K., 22,2-CHOME, IMABASHI, HIGASHI-KU, OSAKA, JAPON, |
发明人 |
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分类号 |
C01B25/16;C01B25/26;C01B25/38;C09C1/36;C22B34/12;(IPC1-7):01B/ |
主分类号 |
C01B25/16 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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