发明名称 Method of making specimens for an electron microscope
摘要 A method and device for preparing a specimen of material for examination by a particle-optical microscope apparatus such as a high-resolution electron microscope (HREM). The known ion milling technique enables specimens to be made sufficiently thin so as to be electron-transparent, that being a condition for HREM materials examination. However, that results in amorphous material on the surface of the specimen which may cause blurring of the image of the surface and also lead to incorrect materials analysis. In accordance with the invention, the surface of the specimen is subjected, possibly following ion milling, to ion bombardment from a plasma of ionized gas which is formed adjoining such surface. This achieves ion etching of the surface, and consequent reduction of the thickness of the specimen, without formation of disturbing amorphous regions on the surface.
申请公布号 US5563412(A) 申请公布日期 1996.10.08
申请号 US19940328228 申请日期 1994.10.25
申请人 U.S. PHILIPS CORPORATION 发明人 ZANDBERGEN, HENDRIK W.;VAN VEEN, ANTHONIUS
分类号 G01N1/28;G01N1/32;H01J37/20;H01J37/305;(IPC1-7):H01J37/26 主分类号 G01N1/28
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