发明名称 PRODUCTION OF TRIAZINE COMPOUND CRYSTAL HAVING HIGH MELTING POINT
摘要 PROBLEM TO BE SOLVED: To provide a process for obtaining the total amount of a chemically synthesized (RS)-N-[2-(3,5-dimethylphenoxy)-1-methylethyl]-6-(1-fluoro-1- methylethyl)-1,3,5-triazine-2,4-diamine in the form of a high-melting point crystal in high efficiency and provide a high-melting point crystal produced by the process. SOLUTION: This process for the production of a high-melting point crystal comprises the addition of a chemically synthesized (RS)-N-[2-(3,5- dimethylphenoxy)-1-methylethyl]-6-(1-fluoro-1-methylethyl)-1,3,5-triaz ine-2,4-diamine crystal to a mixture of a poor solvent and a good solvent of the diamine and heat-treating the obtained mixture at >=30 deg.C and below the melting point of the low-melting point crystal. The high-melting point crystal is produced by this process.
申请公布号 JP2000336079(A) 申请公布日期 2000.12.05
申请号 JP19990147714 申请日期 1999.05.27
申请人 IDEMITSU KOSAN CO LTD 发明人 MURAMOTO TAKAHISA;MATSUNAMI HIDEHIRO
分类号 C07D251/18;A01N43/68;(IPC1-7):C07D251/18 主分类号 C07D251/18
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