发明名称 METHOD OF MAKING ELECTROLUMINESCENT PHOSPHORS WITH SMALL PARTICLE SIZES AND POWDER WITH D50 VALUE OF NO MORE THAN 10 MICROMETERS
摘要 An electroluminescent phosphor powder includes copper-activated zinc sulfide particles that have a size distribution with a D50 value of no more than 10 mum, where no more than 25% of the particles have a size greater than about 15 mum and/or a 24-hr brightness of at least 15 footlamberts. These particles are made by a method that includes first firing copper-doped zinc sulfide mixed with zinc oxide, sulfur and a chloride-containing flux, rapidly cooling the mixture to below 100° C., and then mulling and second firing the mixture to provide a powder. The powder can then be elutriated to provide the electroluminescent powder with a narrow particle size distribution (more than 90% between about 5 and 15 mum). The elutriating step can be avoided (albeit with a slightly wider size distribution) by more tightly controlling the first firing temperature.
申请公布号 US2006220546(A1) 申请公布日期 2006.10.05
申请号 US20050907358 申请日期 2005.03.30
申请人 OSRAM SYLVANIA INC. 发明人 CHEN XIANZHONG;NORTHROP SHELLIE K.
分类号 H05B33/00 主分类号 H05B33/00
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