发明名称 PRODUCTION OF FURFURAL FROM XYLOSE
摘要 Described is a method for producing furfural from one or more substances selected from the group consisting of xylose, oligosaccharides comprising xylose units and polysaccha-rides comprising xylose units.
申请公布号 US2016304481(A1) 申请公布日期 2016.10.20
申请号 US201415103336 申请日期 2014.12.10
申请人 BASF SE 发明人 Koch Stefan;Kindler Alois
分类号 C07D307/50 主分类号 C07D307/50
代理机构 代理人
主权项 1. Method for producing furfural comprising providing an aqueous feed mixture comprising: (i) one or more substances selected from the group consisting of xylose, oligosaccharides comprising xylose units, and polysaccharides comprising xylose units (ii) methanesulfonic acid (iii) one or more salts wherein the total concentration of (iii) said one or more salts is in the range of from 0.5 wt.-% to 20 wt.-% based on the total weight of said aqueous feed mixture, contacting said aqueous feed mixture with an extraction liquid comprising one or more organic solvents, wherein said one or more solvents have a higher solubility for furfural than said aqueous feed mixture andare selected so that when said aqueous feed mixture is contacted with said extraction liquid two separate liquid phases are formed, wherein in a first liquid phase the concentration of water is higher than the concentration of said organic solvents and in a second liquid phase the concentration of said organic solvents is higher than the concentration of water subjecting said aqueous feed mixture while contacted with said extraction liquid to a thermal treatment so that said one or more substances selected from the group consisting of xylose, oligosaccharides comprising xylose units, and polysaccharides comprising xylose units are reacted to furfural which is extracted from said aqueous feed mixture into said extraction liquid.
地址 Ludwigshafen DE