发明名称 |
POLYCRYSTALLINE SILICON ROD, PRODUCTION METHOD THEREFOR, AND FZ SILICON SINGLE CRYSTAL |
摘要 |
In the present invention, from a region from the center (r = 0) to R/3 of a polycrystalline silicon rod, a plate-shaped sample having as a main surface a cross-section of the polycrystalline silicon rod which is orthogonal to the diameter direction thereof is collected. The plate-shaped sample is disposed at a position where a Bragg reflection from a face of Miller indices (111) is detected. The plate-shaped sample is rotated in-plane by a rotation angle Φ with the center of the plate-shaped sample serving as the rotation center in such a manner that an X-ray irradiation region defined by a slit performs a Φ scan on the main surface of the plate-shaped sample, and a diffraction chart showing the dependency, on the plate-shaped sample rotation angle, of the intensity of the Bragg reflection from the face of Miller indices (111) is determined. A ratio (Sp/St) is calculated between a surface area Sp of a peak portion that has appeared in the diffraction chart and the total surface area St of the diffraction chart. A polycrystalline silicon rod with a surface area ratio Sp/St evaluated by the above procedure that is 2% or less is selected. |
申请公布号 |
WO2016132411(A1) |
申请公布日期 |
2016.08.25 |
申请号 |
WO2015JP06156 |
申请日期 |
2015.12.10 |
申请人 |
SHIN-ETSU CHEMICAL CO., LTD. |
发明人 |
MIYAO, Shuichi;NETSU, Shigeyoshi |
分类号 |
C01B33/02;C30B29/06 |
主分类号 |
C01B33/02 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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