| 摘要 |
The invention relates to a process for preparing caprolactam by admixture of cyclohexanone oxime to a reaction mixture comprising caprolactam and sulfuric acid using a mixing device, said mixing device comprising (i) a tube through which the reaction mixture can flow, and (ii) channels disposed around the tube, said channels opening into the tube, said process comprising: passing the reaction mixture through the tube, and feeding the cyclohexanone oxime into the reaction mixture through one or more of said channels, wherein Re > 5000, Re being the Reynolds number as defined by &rgr;V.D/&eegr;, wherein &rgr; = density (in kg/m) of the reaction mixture that is fed to the tube, V = velocity of the reaction mixture, V being defined as W/A, wherein W is the flow rate (in m/s) of the reaction mixture that is fed into the tube and A is the cross section area of the tube (in m) at the level where said channels open into the tube, D = diameter of the tube at the level where said channels open into the tube (in m), &eegr; = viscosity of the reaction mixture that is fed into the tube (in Pa.s). |
