主权项 |
1. A method of encapsulating particulate materials absent catalyst and solvent, the method consisting of:
a. providing acidified water at least sufficient for hydrolyzing a predetermined amount of alkoxysilane; b. thereafter dispersing at least one type of particulate material in the acidified water; c. thereafter slowly adding a predetermined amount of alkoxysilane having the general formula:
RxSi(OR′))4-x wherein R is selected from the group consisting essentially of alkyl groups, substituted alkyl groups, aryl groups, substituted aryl groups, vinyl, allyl, and hydrogen, wherein the substituents are selected from the group consisting of fluorine, amino, hydroxy, and combinations thereof, and wherein R′ is selected from hydrogen and alkyl groups of 1 to 4 carbon atoms; d. thereafter allowing sufficient time for the alkoxysilane to hydrolyze and build a predetermined particle size. |