INTEGRATED PROCESS AND APPARATUS FOR RECOVERY OF HELIUM RICH STREAMS

摘要

The present invention relates a process and apparatus that recovers a helium rich stream from a mixed gas having low concentrations of helium therein. More specifically, the invention relates to an integrated process and apparatus for treating a mixed feed gas from an operating process that produces a fluid product from natural gas containing helium, such as processes that produce ammonia, methanol, or liquid hydrocarbons.

主权项

1. An integrated system for recovery of a helium rich stream and a hydrogen rich stream from a feed stream containing 10-80 volume percent hydrogen, 0.1-5.0 volume percent helium, and the balance higher boiling components, comprising:
(a) routing a compressed and warmed feed stream to a first hydrogen transport membrane system having one or more hydrogen transport membranes for carrying out the bulk separation between a first hydrogen permeate stream and a first helium-containing retentate stream; (b) cooling and routing the first helium-containing retentate stream to a size selective polymeric membrane system having one or more polymeric membrane stages to remove the higher boiling components and to produce a resulting second permeate stream composed of primarily hydrogen and helium and a second retentate stream; (c) compressing the resulting second permeate stream in step (b) and feeding same to a second hydrogen transport membrane system having one or more hydrogen transport membranes to further recover one or more hydrogen permeate streams and a helium rich retentate product having about 80% helium or higher volume by content.