发明名称 |
HOLLOW SILICA MICROCAPSULE HAVING ZEOLITE WALL MATERIAL AND METHOD FOR MANUFACTURING THE SAME |
摘要 |
PROBLEM TO BE SOLVED: To provide hollow silica microcapsules having a narrow pore diameter distribution and using a pore forming wall material having a zeolite structure. SOLUTION: The hollow silica microcapsules are manufactured through (A) a step of obtaining a W/O type emulsion by mixing an aqueous solution containing a silicate of an alkali metal with an organic solvent and a surfactant; (B) a step of forming hollow silica microcapsules by mixing the obtained emulsion with an aqueous solution containing the ammonium salt of an inorganic acid or the like; (C) a step of washing the hollow silica microcapsules with water without carrying out alcohol cleaning and then drying and firing those; (D) a step of impregnating an aqueous solution containing a structure regulating agent into the fired hollow silica microcapsules; (E) a step of carrying out a hydrothermal synthesis reaction by heating the hollow silica microcapsules with the impregnated aqueous solution containing the structure regulating agent to a crystallization temperature of the zeolite; and (F) a step of removing the structure regulating agent from the hollow silica microcapsules after the hydrothermal synthesis reaction. COPYRIGHT: (C)2007,JPO&INPIT |
申请公布号 |
JP2006265019(A) |
申请公布日期 |
2006.10.05 |
申请号 |
JP20050083440 |
申请日期 |
2005.03.23 |
申请人 |
SHIGA PREF GOV;NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL & TECHNOLOGY |
发明人 |
NAKADA KUNIHIKO;FUJIWARA MASAHIRO |
分类号 |
C01B33/12;B01J13/04;B01J13/20 |
主分类号 |
C01B33/12 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|