| 摘要 |
2,2',4,4',6,6'-hexanitrobibenzyl, an intermediate compound used for making hexanitrostilbene, is prepared by adding an aqueous alkaline metal hypochlorite solution containing an alkaline metal hydroxide to trinitrotoluene dispersed in a single solvent selected from the group consisting of methanol, ethanol, 2-methoxyethanol, isopropanol, acetone, tetrahydrofuran, N,N-dimethylformamide, N,N-dimethylacetamide, pyridine and N-methyl pyrrolidinone. The compound is then separated from the reaction mixture.
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