发明名称 PREPARATION OF N-PERFLUOROALKYL-N- HYDROXYARENESULFONAMIDE
摘要 PURPOSE:To obtain the titled compound useful as a herbicide in high yield, by reacting a perfluoronitrosalkane with an arenesulfonic acid. CONSTITUTION:A perfluoronitrosalkane of the formula Rf-NO (Rf is lower perfluoroalkyl) is reacted with an arenesulfonic acid of the formula ArSO2H (Ar is substituted or unsubstituted aryl) to give the aimed N-perfluoroalkyl-N-hydroxyarenesulfonamide of formula I in high reaction yield. THF, dimethyl ether, DMF, DMSO, etc. are preferred for a reaction solvent, and the reaction temperature is preferably -100-+70 deg.C.
申请公布号 JPS60166659(A) 申请公布日期 1985.08.29
申请号 JP19840022013 申请日期 1984.02.10
申请人 SAGAMI CHUO KAGAKU KENKYUSHO 发明人 UMEMOTO TERUO
分类号 C07C311/49;C07C67/00;C07C301/00;C07C303/36 主分类号 C07C311/49
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