发明名称 PRODUCTION OF 2-PHENYL-ETHYLENE-PHOSPHONIC ACID DICHLORIDE
摘要 PURPOSE:To obtain the titled compound useful as an additive for the binder of molding sand, without producing by-product, by reacting styrene with phosphorus pentachloride in an inert solvent and adding and reacting phthalic anhydride to the resultant reaction mixture. CONSTITUTION:Styrene is made to react with phosphorus pentachloride in an inert solvent (preferably benzene or toluene) preferably at 50-80 deg.C. The objective compound is produced by adding phthalic anhydride to the reaction mixture and reacting preferably at 50-80 deg.C for 1-20hr. The molar ratio of phosphorus pentachloride and phthalic anhydride to styrene is preferably 1-3 to 1.
申请公布号 JPS63145289(A) 申请公布日期 1988.06.17
申请号 JP19860293012 申请日期 1986.12.09
申请人 NISSAN CHEM IND LTD 发明人 YOSHIOKA YOSHIKAZU;SUZUKI FUMIO;MASUMORI MAKOTO;HASHIBA ISAO
分类号 B22C1/20;C07F9/42 主分类号 B22C1/20
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