发明名称 AN IMPROVED PROCESS FOR PURIFYING ALPHA-KETO ACIDS
摘要 The present invention relates to an improved process for purifying .alpha.-keto acids. In particular, the present invention pertains to the isolation of pivalic acid and other organic impurities from .alpha.-keto acids. The process of the invention generally includes (i) the partial acidification of an aqueous solution of a sodium salt of the .alpha.-keto acid (a"keto salt"), (ii) a first solvent extraction of the keto salt solution to remove organic impurities, (iii) further acidification of the keto salt solution, (iv) a second solvent extraction to remove the .alpha.-keto acid, and (v) isolation of the .alpha.-keto acid from the solvent. In a preferred embodiment, the present invention relates to the preparation of trimethylpyruvic acid (TMPA) of enhanced purity.
申请公布号 CA2307989(A1) 申请公布日期 2000.11.19
申请号 CA20002307989 申请日期 2000.05.10
申请人 BAYER CORPORATION 发明人 HOWERTON, CATHY L.;JACKMAN, DENNIS E.
分类号 C07C51/41;C07C51/48;(IPC1-7):C07C59/185 主分类号 C07C51/41
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