Method of measuring amount of chemical cure and amount of surface contamination using infrared absorbance

摘要

Amount of coating cure or contamination is determined. An infrared beam is transmitted into a crystal. The beam reflects off an internal face at an angle higher than critical reflection angle to generate total reflection at the crystal face. The beam exits the crystal, is filtered at two wavelengths, and is detected to give values I_o1 and I_o2 of infrared energy reflected without coating. A coated sample contacts an outside face of the crystal. An evanescent wave penetrates the sample where the beam reflects from internal crystal face. The beam is partially absorbed by sample, exits the crystal, is filtered at two wavelengths, and is detected to give values I_c1 and I_c2 of infrared energy reflected with coating. Absorbance values A 1 and A 2 at two wavelengths are A 1 =-log₁₀(I_c1/I_o1) and A 2 =-log₁₀(I_c2/I_o2). Amount of cure or contamination is proportional to ratio or difference between A 1 and A 2.