发明名称 METHOD FOR PREPARING DERIVATIVES OF 4,4'-DIAMINOSTILBENE-2,2'-DISULFOACID
摘要 FIELD: organic chemistry, chemical technology. SUBSTANCE: invention describes method for preparing derivatives of 4,4'-diaminostilbene-2,2'-disulfoacid as stable aqueous solutions. Method involves interaction of cyanuric chloride with 4,4'-diaminostilbene-2,2'-disulfoacid and amine of the formula (II): wherein R means hydrogen atom, SO3M, wherein M means sodium, potassium, mono-, di-, triethanolamine in an aqueous medium followed by isolation of the interaction product by effect with organic or inorganic acid at 50-90 C and conversion of free acid to solution by effect with inorganic base or ethanolamine at 60-80 C in the presence of carbamide, glycol and ethanolamine. Compounds are used as optical bleach agents in paper and pulp and textile industry. EFFECT: improved preparing method.2 cl
申请公布号 RU2223957(C2) 申请公布日期 2004.02.20
申请号 RU20010132053 申请日期 2001.11.28
申请人 发明人 MITIN N.A.;KIRO Z.B.;MAKRIDIN N.A.;TEREKHOV A.I.;UTROBIN A.N.
分类号 C07D251/68 主分类号 C07D251/68
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