发明名称 Detection of trace amounts of perchlorate using SERS-active capture matrices
摘要 A perchlorate detector comprising: surface-enhanced Raman spectroscopy (SERS)-active, magnetic, capture matrices that are selective for perchlorate, wherein the capture matrices are designed to be added to a sample solution; a detection chamber configured to hold the sample solution and the capture matrices; a selectively engageable magnet assembly coupled to the detection chamber such that when the magnet assembly is engaged or disengaged the capture matrices are respectively confined or not confined to a confinement region of the detection chamber; and a Raman spectrometer optically aligned with the confinement region of the detection chamber and configured to interrogate the capture matrices when the magnet assembly is engaged in order to detect and determine a concentration of perchlorate bound to the capture matrices.
申请公布号 US9470671(B1) 申请公布日期 2016.10.18
申请号 US201514719114 申请日期 2015.05.21
申请人 The United States of America as represented by Secretary of the Navy 发明人 Boss Pamela A.;Putnam Michael D.
分类号 G01N33/18;G01N21/65;B01J19/00;G01N27/333 主分类号 G01N33/18
代理机构 SPAWAR Systems Center Pacific 代理人 SPAWAR Systems Center Pacific ;Eppele Kyle;Anderson J. Eric
主权项 1. A perchlorate detector comprising: surface-enhanced Raman spectroscopy (SERS)-active, magnetic, capture matrices that are selective for perchlorate, wherein the capture matrices are designed to be added to a sample solution; a detection chamber configured to hold the sample solution and the capture matrices wherein the detection chamber comprises a confinement region having an indentation; a selectively engageable magnet assembly coupled to the detection chamber such that when the magnet assembly is engaged or disengaged the capture matrices are respectively confined or not confined to the confinement region of the detection chamber; a Raman spectrometer optically aligned with the confinement region of the detection chamber and configured to interrogate the capture matrices when the magnet assembly is engaged in order to detect and determine a concentration of perchlorate bound to the capture matrices; and a water reservoir hydraulically coupled to the indentation via a valve such that when the valve is open and the magnetic assembly is disengaged water enters the indentation and flushes the capture matrices out of the indentation.
地址 Washington DC US