VERFAHREN ZUR SPEKTROMETRISCHEN ANALYSE EINER ORGANOMETALLISCHEN ZUSAMMENSETZUNG.

摘要

A method of analyzing a volatile, air or moisture sensitive or pyrophoric, liquid, organometallic compound for an impurity comprising inserting a sample of the compound into an exponential dilution flask (10), allowing substantially the entire sample to vaporize, and analyzing the vapor by plasma spectroscopy; or decomposing the sample by drop-wise addition into frozen aqueous acid, diluting the decomposed sample with water, and analyzing the diluted, decomposed sample by plasma spectroscopy.