发明名称 |
Intermediate in the process for the preparation of trans-{66 {hu 9{b -isoambrettolide |
摘要 |
A process is described for producing trans- DELTA 9-isoambrettolide from aleuritic acid in three reaction steps; first forming a dioxolane by treatment with an excess amount of an orthoformate or a dialkyl formamide dialkyl acetal; then forming the corresponding bengalene acid derivative by heating the dioxolane with acetic anhydride; and then cyclizing the resulting trans bengalene acid derivative by heating it, thereby yielding a high quality substantially pure or 100% pure trans- DELTA 9-isoambrettolide.
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申请公布号 |
US4014902(A) |
申请公布日期 |
1977.03.29 |
申请号 |
US19760694452 |
申请日期 |
1976.06.09 |
申请人 |
INTERNATIONAL FLAVORS & FRAGRANCES INC. |
发明人 |
TSENG, CHING Y. |
分类号 |
C07D313/00;C07D315/00;C11B9/00;(IPC1-7):C07D317/10 |
主分类号 |
C07D313/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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