发明名称 METHOD FOR EXTRACTION OF AMINONAPHTHOLSULFOACIDS AND AMINOPHENOLSULFOACIDS FROM AQUEOUS SOLUTIONS
摘要 FIELD: organic chemistry, analytical chemistry, chemical technology. ^ SUBSTANCE: method for extraction of aminonaphtholsulfoacids and aminophenolsulfoacids involves extraction with organic solvent wherein sodium dodecyl sulfate an aqueous solution is added to aqueous solution up to its concentration 1.5 x 10-4 mol/dm3, hydrochloric acid is added up to the concentration 1.5-1.6 mol/dm3. As extractant method involves using 1,4-dioxane in the volume ratio of extractant to sample = 1:10 and extraction is carried out from saturated solution of ammonium sulfate. Invention provides enhancing degree of extraction of aminonaphtholmonosulfoacids and aminophenolmonosulfoacids from aqueous solutions wherein extraction degree of sulfoacids is 96.1-99.6% after a single extraction. Invention can be recommended for concentrating 1-amino-2-naphthol-4-sulfoacid and 2-aminophenol-4-sulfoacid from treated sewage waters in manufacturing azodyes. ^ EFFECT: improved method for extraction. ^ 1 tbl, 11 ex
申请公布号 RU2258698(C1) 申请公布日期 2005.08.20
申请号 RU20040121391 申请日期 2004.07.12
申请人 发明人 KORENMAN JA.I.;GUBIN A.S.;SUKHANOV P.T.
分类号 C07C303/44;B01D11/04;C07C309/50 主分类号 C07C303/44
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