摘要 |
Elemental titanium is produced by reducing titanium tetrachloride using an alkali or alkaline earth metal, preferably sodium. The reaction is carried out in the vapour phase, a carrier gas, preferably hydrogen, being heated by an electric arc and injected into the reaction chamber to heat the sodium and titanium tetrachloride which are injected as liquids or vapours. The reaction is carried out at a temperature above the melting point of titanium, typically between 1,800 DEG and 2,500 DEG C, the titanium falling as a liquid to the bottom of the reaction chamber and the chloride of the reducing metal and other unwanted products being removed in vapour form. The chloride of the reducing metal is passed through a heat exchanger for heating material passing into the chamber and is electrolysed to provide the required alkali or alkaline earth metal.
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