| 发明名称 |
METHOD FOR MANUFACTURING HEXAGONAL PLATE-SHAPED ZINC OXIDE PARTICLES |
| 摘要 |
A method of producing hexagonal plate-like zinc oxide particles having a sharp particle size distribution (i.e., a relatively uniform particle size) at a high weight yield and a high percent yield is provided. The method of producing hexagonal plate-like zinc oxide particles of the present invention comprises mixing by stirring an aqueous hexamethylenetetramine (HMT) solution, a solution of an anionic surfactant in a water-insoluble organic solvent, and optionally water to form a microemulsion containing an aqueous phase of an aqueous hexamethylenetetramine solution having a molar concentration of 0.05 M or more; dropwise adding an aqueous zinc salt solution to the microemulsion; and heating the microemulsion containing the aqueous zinc salt solution to a reaction temperature of 80° C. or more without using any autoclave to form hexagonal plate-like zinc oxide particles. |
| 申请公布号 |
US2017044022(A1) |
申请公布日期 |
2017.02.16 |
| 申请号 |
US201615336937 |
申请日期 |
2016.10.28 |
| 申请人 |
NGK INSULATORS, LTD. ;NAGOYA INSTITUTE OF TECHNOLOGY |
发明人 |
YOSHIKAWA Jun;NANATAKI Tsutomu;HAYAKAWA Tomokatsu |
| 分类号 |
C01G9/02 |
主分类号 |
C01G9/02 |
| 代理机构 |
|
代理人 |
|
| 主权项 |
1. A method of producing hexagonal plate-like zinc oxide particles, comprising:
mixing by stirring an aqueous hexamethylenetetramine (HMT) solution, a solution of an anionic surfactant in a water-insoluble organic solvent, and optionally water to form a microemulsion containing an aqueous phase of an aqueous hexamethylenetetramine solution having a molar concentration of 0.05 M or more; dropwise adding an aqueous zinc salt solution to the microemulsion; and heating the microemulsion containing the aqueous zinc salt solution to a reaction temperature of 80° C. or more without using any autoclave to form hexagonal plate-like zinc oxide particles. |
| 地址 |
Nagoya-Shi JP |
