PREPARATION PROCESS AND PRODUCT OF DIALKYL PHOSPHINATE

摘要

The present provides a process for preparing dialkyl phosphinate, comprising: (1) firstly adding 0-99% of the total weight of phosphinic acids and/or salts thereof and a solvent into a reaction kettle;(2) in the reaction kettle in the presence of alkene and initiator, continuously adding 1-100% of the total weight of the phosphinic acids and/or salts thereof into the reaction system, during the addition process, when the mole contents of monoalkyl phosphinic acids and/or salts thereof account for 10% or less of the total molar contents of phosphorus in the reaction system, stopping adding the phosphinic acids and/or salts thereof. Also providing a dialkyl phosphinate flame retardant prepared by above preparation process.