发明名称 |
METHOD TO PURIFY FERULC ACID AND/OR SALTS THEREOF |
摘要 |
Methods to purify ferulic acid and/or salts thereof, both in solid state as in solution, said methods include: dissolve the ferulic acid, with a selective organic solvent, recover and isolate the solution from the insoluble impurities with filters; recover the organic solvent evaporating the solution; mix the concentrated extract of ferulic acid with water to pre-crystallize the hydrosoluble impurities; evaporate the mixture to remove the remains of the organic solvent; concentrate the mixture free of solvent in an evaporator; cool the mixture down to 40 °C; let the concentrated mixture set for 1 h, to then isolate by sedimentation the water-insoluble impurities; re-heat the mixture free of impurities to 70 °C; purify the mixture through a synthetic resin, transfer the purified mixture to a crystallizing container to crystallize the ferulic acid; remove the mother liquor of crystallization of the precipitate of ferulic acid; dry the ferulic acid. |
申请公布号 |
CA2902089(A1) |
申请公布日期 |
2017.01.24 |
申请号 |
CA20152902089 |
申请日期 |
2015.07.24 |
申请人 |
LABORATORIOS MINKAB, S.A. DE C.V. |
发明人 |
ASAFF ARANCIBIA, JORGE SELIM;ACEVES DIEZ, ANGEL EMILIO;HERRERA HERRERA, RUBEN;ALEJO CASTILLO, MARIA LUCIA |
分类号 |
C07C51/42;C07C59/64 |
主分类号 |
C07C51/42 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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