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发明名称
一种微波辅助热解制备纳米ZnO的方法
摘要
本发明提供了一种微波辅助热解制备纳米ZnO的方法,该方法首先将十八胺加热熔融,然后加入硝酸锌;再通过微波辅助热解的方式制备纳米ZnO。该方法操作简单、绿色环保。
申请公布号
CN106186041A
申请公布日期
2016.12.07
申请号
CN201610527695.8
申请日期
2016.07.06
申请人
常州大学
发明人
彭勇刚;纪俊玲;陶永新;汪媛
分类号
C01G9/02(2006.01)I
主分类号
C01G9/02(2006.01)I
代理机构
代理人
主权项
一种微波辅助热解制备纳米ZnO的方法,其特征在于:步骤如下:将30‑100g十八胺加热到100℃,待其完全溶解后加入0.2‑1.0g Zn(NO<sub>3</sub>)<sub>2</sub>·6H<sub>2</sub>O,不断搅拌,待溶质完全溶解后,将反应液置于微波反应器内,微波加热至180‑220℃,保温30‑60min,保温结束后,收集沉淀物,沉淀物分别用无水乙醇、蒸馏水洗涤3‑5次,60‑80℃烘干,即得纳米ZnO。
地址
213164 江苏省常州市武进区滆湖路1号
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