发明名称 有機色素MK−2の製造方法
摘要 PROBLEM TO BE SOLVED: To provide a method for producing an organic coloring matter MK-2 in a short period of time and in a good yield.SOLUTION: The method for producing an organic coloring matter MK-2 comprises: a first step of coupling 3-hexylthiophene in the presence fo an iodine catalyst and an activator to synthesize a thiophene dimer having two thiophene molecules bonded (H-T bithiophene); a second step of halogenating a 5-position of the resultant H-T bithiophene; a third step of substituting halogen at a 5-position of the resultant halogenated H-T bithiophene with a 9-ethylcarbazolyl group; a fourth step of halogenating a 5'-position of the resultant 9-ethylcarbazolyl H-T bithiophene; a fifth step of bonding H-T bithiophene to the resultant halogenated body to form a thiophene tetramer; a sixth step of folmylating a thiophene terminal of the resultant thiophene tetramer; and a seventh step of reacting the resultant formylated body with a cyanoacetic acid to produce the MK-2.
申请公布号 JP5963167(B2) 申请公布日期 2016.08.03
申请号 JP20120188699 申请日期 2012.08.29
申请人 学校法人立命館 发明人 北 泰行;土肥 寿文
分类号 C09B23/00 主分类号 C09B23/00
代理机构 代理人
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