发明名称 GARNET SINGLE CRYSTAL AND METHOD FOR PRODUCING THE SAME
摘要 [Object] To provide a high-quality, transparent garnet single crystal with suppressed cell growth that would otherwise lead to partially inhomogeneous crystal composition, and a method for producing the garnet single crystal. [Solving means] The garnet single crystal is grown by bringing a seed crystal into contact with a raw-material melt in a crucible disposed inside a chamber and pulling, while rotating, the seed crystal. The garnet single crystal is characterized by being represented by a general formula: (Tb3-xScx) (Sc2-yAly)Al3O12-z (provided that 0.11≦x≦0.14, and 0.17≦y≦0.23). The garnet single crystal is grown as follows. First, a mixture powder containing 20.9 to 21.2% by mole terbium oxide, 32.7 to 33.3% by mole scandium oxide, and the balance of aluminium oxide and unavoidable impurities is filled into the crucible and melted. Then, while a nitrogen gas is supplied into the chamber, the number of rotations of the seed crystal is set to 5 to 20 rpm, and the rate of pulling the seed crystal is set to 0.3 to 0.8 mm/h for the growth.
申请公布号 US2016145765(A1) 申请公布日期 2016.05.26
申请号 US201414787954 申请日期 2014.03.20
申请人 SUMITOMO METAL MINING CO., LTD 发明人 MATSUI Masayoshi;TATSUMIYA Kazuki;ISHIDA Fumiaki
分类号 C30B15/30;G02F1/09;G02F1/00;C30B29/20 主分类号 C30B15/30
代理机构 代理人
主权项 1. A garnet single crystal characterized in that the garnet single crystal is represented by the following general formula: (Tb3-xScx)(Sc2-yAly)Al3O12-z  (1) (where x satisfies 0.11≦x≦0.14, and y satisfies 0.17≦y≦0.23).
地址 Tokyo JP