发明名称 ACETIC ACID PRODUCTION METHOD
摘要 Acetic acid is produced while inhibiting an increased concentration or production of hydrogen iodide in a flash evaporator. A process for producing acetic acid comprises a series of steps: a reaction step for continuously allowing methanol to react with carbon monoxide in the presence of a catalyst system comprising a metal catalyst, an ionic iodide, and methyl iodide in a carbonylation reactor, a flash distillation step for continuously feeding a flasher with a reaction mixture from the reactor and evaporating a volatile component at least containing product acetic acid, methyl acetate, and methyl iodide by flash distillation to separate the volatile component and a liquid catalyst mixture at least containing the metal catalyst and the ionic iodide, and an acetic acid collection step for separating a stream containing acetic acid from the volatile component to collect acetic acid; wherein, in the flash distillation step, the flash distillation is conducted under the condition that the concentration of methyl acetate in the liquid catalyst mixture is not less than 0.6% by weight.
申请公布号 EP2653460(A4) 申请公布日期 2016.05.25
申请号 EP20110848297 申请日期 2011.12.01
申请人 DAICEL CORPORATION 发明人 SHIMIZU MASAHIKO;SAITO RYUJI;MIURA HIROYUKI;UENO TAKASHI;NAKAJIMA HIDEHIKO
分类号 C07C51/44;B01J23/46;B01J27/13;C07B61/00;C07C51/12;C07C53/08 主分类号 C07C51/44
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