发明名称 PZT系強誘電体薄膜の製造方法
摘要 [Task] To obtain a dense PZT-based ferroelectric thin film having excellent crystal orientation in which cracking or a decrease in the film density does not occur even when a thick film having a film thickness per layer of 100 nm or more is coated, calcined, and fired using a CSD method. [Means for Resolution] When a PZT-based ferroelectric thin film is manufactured on a lower electrode by coating, calcining, and then firing so as to crystallize a PZT-based ferroelectric thin film-forming composition on the lower electrode of a substrate having the lower electrode in which the crystal plane is oriented in a (111) axis direction, the PZT-based ferroelectric thin film-forming composition is coated on the surface of the lower electrode using a CSD method, and calcination is slowly carried out on a formed sol film in a temperature pattern including a first holding step in which the temperature of the composition is increased frog a predetermined temperature such as room temperature using infrared rays and the composition is held at a temperature in a range of 200°C to 350°C and a second holding step in which the temperature of composition is increased from the holding temperature of the first holding step and is held at a temperature in a range of 350°C to 500°C higher than the holding temperature of the first holding step.
申请公布号 JP5919956(B2) 申请公布日期 2016.05.18
申请号 JP20120078916 申请日期 2012.03.30
申请人 三菱マテリアル株式会社 发明人 土井 利浩;桜井 英章;渡辺 敏昭;曽山 信幸
分类号 H01L21/316;C01G25/00;H01G4/12;H01G4/33;H01L21/336;H01L21/8246;H01L27/105;H01L29/788;H01L29/792;H01L41/09;H01L41/18;H01L41/187;H01L41/43 主分类号 H01L21/316
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