发明名称 METHOD FOR MANUFACTURING SILVER PARTICLES
摘要 The present invention provides a method for producing silver particles, the method capable of adjusting the particle diameter to be within the range of several tens of nanometers to several hundreds of nanometers and also producing silver particles with a uniform particle diameter. The present invention relates to a method for producing silver particles by heating of a reaction system containing a thermally-decomposable silver-amine complex precursor, including a process of producing a silver-amine complex, a process of adding an organic compound having an amide (carboxylic amide) as a skeleton to a reaction system, and a process of heating the reaction system, in which a water content in the reaction system before the heating is 20 to 100 parts by weight relative to 100 parts by weight of the silver compound. The present invention can produce uniform silver particles while the particle diameter is controlled.
申请公布号 US2016121404(A1) 申请公布日期 2016.05.05
申请号 US201414891725 申请日期 2014.05.20
申请人 TANAKA KIKINZOKU KOGYO K.K. 发明人 MAKITA Yuichi;OHSHIMA Yuusuke;MATSUDA Hidekazu;NAKAMURA Noriaki;TANIUCHI Junichi;KUBO Hitoshi
分类号 B22F9/30;B22F1/00 主分类号 B22F9/30
代理机构 代理人
主权项 1. A method for producing silver particles by use of a thermally-decomposable silver-amine complex as a precursor and heating of a reaction system containing the precursor, comprising: a process (a): mixing a thermally-decomposable silver compound with an amine to produce a silver-amine complex as a precursor; a process (b): adding an organic compound, which has an amide as a skeleton, represented by a following formula to a reaction system (R is hydrogen, hydrocarbon, an amino group, or a combination thereof; R′ and R″ are hydrogen or hydrocarbon); and a process (c): heating the reaction system, wherein a water content in the reaction system before the heating in the process (c) is 20 to 100 parts by weight relative to 100 parts by weight of the silver compound.
地址 Tokyo JP