发明名称 |
Crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[B][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione |
摘要 |
The present invention relates to a novel crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione The invention also relates to a process for the production of this crystalline form and formulations for plant protection which contains the novel crystalline form of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione. |
申请公布号 |
US9328101(B2) |
申请公布日期 |
2016.05.03 |
申请号 |
US201314402496 |
申请日期 |
2013.05.15 |
申请人 |
BASF SE |
发明人 |
Reinhard Robert;Chiodo Tiziana;Wolf Bernd;Scherer Stefan;Bratz Matthias;Witschel Matthias;Newton Trevor William;Seitz Thomas |
分类号 |
A01N43/84;C07D413/04 |
主分类号 |
A01N43/84 |
代理机构 |
Brinks Gilson & Lione |
代理人 |
Brinks Gilson & Lione |
主权项 |
1. A crystalline form B of 1,5-dimethyl-6-thioxo-3-(2,2,7-trifluoro-3-oxo-4-(prop-2-ynyl)-3,4-dihydro-2H-benzo[b][1,4]oxazin-6-yl)-1,3,5-triazinane-2,4-dione, which in an X-ray powder diffraction diagram at 25° C. and Cu-Kα radiation displays at least 3 of the following reflections, quoted as 20 values: 9.0±0.2°, 10.9±0.2°, 11.5±0.2°, 12.9±0.2°, 13.5±0.2°, 14.9±0.2°, 16.4±0.2°, 16.5±0.2°, 17.5±0.2° and 20.3±0.2°. |
地址 |
Ludwigshafen DE |