| 发明名称 | Stepwise execution of exothermic reactions with participation of carbocations | ||
| 摘要 | The invention relates to a method for carrying out reactions with participation of carbocations, whereby the initial most strongly exothermic phase of the reaction is carried out at high temperature (60 to 120° C.) and short residence time (1 to 30 seconds) in a microreactor and the subsequent less exothermic phases are carried out at optionally lower temperatures in two or more residence time units with longer residence times (1 to 30 seconds). | ||
| 申请公布号 | US9327263(B2) | 申请公布日期 | 2016.05.03 |
| 申请号 | US200611920847 | 申请日期 | 2006.04.26 |
| 申请人 | ESIM Chemicals GmbH | 发明人 | Pöchlauer Peter;Kotthaus Martina;Vorbach Martin;Deak Martin;Zich Thomas;Marr Rolf |
| 分类号 | C07C231/06;B01J19/00;B01J19/18;B01J19/24;B01F13/00;F28D21/00 | 主分类号 | C07C231/06 |
| 代理机构 | Pierce Atwood LLP | 代理人 | Pierce Atwood LLP ;Arner Raymond G. |
| 主权项 | 1. An improved process for the execution of a reaction with participation of carbocations, which comprises: (a) carrying out a most strongly exothermic initial phase of the reaction in a microreactor at a high temperature of from 60 to 120° C. and a short residence time of 1 to 30 seconds, and then subsequently (b) carrying out less exothermic phases of the reaction in two or more residence time units, wherein the residence time in a first residence time unit is from 1 to 30 minutes and the reaction temperature in the first residence time unit is lower by 5 to 30° C. than the microreactor. | ||
| 地址 | Linz AT | ||