发明名称 TETRAHYDROFURAN-2,5-DICARBALDEHYDES (DIFORMYL-TETRAHYDROFURAN, DFTHF) AND PROCESS FOR MAKING THE SAME
摘要 Tetrahydrofuran-(THF)-2,5-dicarbaldehyde and a process of preparing the same are described. The process involves reacting THF-diols in an inert organic solvent with an oxidizing agent at a temperature up to about 50 C. The process can use either HMF or THF-diols as starting materials, and enables a single-step conversion of THF-diols into a precursor material that can be transformed into a multitude of furanic derivative compounds. THF dicarbaldehyde can be modified according to certain reaction processes to generate either new or existing derivative compounds.
申请公布号 US2016096813(A1) 申请公布日期 2016.04.07
申请号 US201414892072 申请日期 2014.06.10
申请人 ARCHER DANIELS MIDLAND COMPANY 发明人 Stensrud Kenneth
分类号 C07D307/24;C07D307/14;C07D307/12 主分类号 C07D307/24
代理机构 代理人
主权项 1. A process of making a tetrahydrofuran-(THF)-2,5-dicarbaldehyde, comprising: providing a reaction mixture containing THF-diols and an inert organic solvent; reacting said THF-diols with an oxidizing agent at a reaction temperature between about 10° C. to about 50° C., in a non-inert atmosphere.
地址 Decatur IL US