发明名称 |
Method for producing 6-chlorodibenzo[D,F] [1,3,2] dioxaphosphepin |
摘要 |
The invention relates to a method for producing 6-chlorodibenzo[d,f][1,3,2]-dioxaphosphepin (formula 1), comprising the following steps: a) addition of 2,2′-dihydroxybiphenyl, which is suspended in an inert solvant. into a reactor to an excess of phosphorous trichloride under inert gas and stirring; b) discharge and neutralization of the resulting gases from the reaction mixture; c) separation of the excess phosphorous trichloride and the solvant; d) obtention of 6-chlorodibenzo[d,f][1,3,2]-dioxaphosphepin. |
申请公布号 |
US9290527(B2) |
申请公布日期 |
2016.03.22 |
申请号 |
US201414219713 |
申请日期 |
2014.03.19 |
申请人 |
EVONIK DEGUSSA GMBH |
发明人 |
Fridag Dirk;Franke Robert;Schemmer Bernhard;Kreidler Burkard;Wechsler Bjoern |
分类号 |
C07F9/6574 |
主分类号 |
C07F9/6574 |
代理机构 |
Oblon, McClelland, Maier & Neustadt, L.L.P. |
代理人 |
Oblon, McClelland, Maier & Neustadt, L.L.P. |
主权项 |
1. A process for preparing 6-chlorodibenzo[d,f]-[1,3,2]dioxaphosphepin, which comprises:
a) adding a suspension of 2,2′-dihydroxybiphenyl in an inert solvent to an excess of phosphorus trichloride under inert gas in a reactor and stirring, to obtain a reaction mixture and resulting gas; b) discharging and neutralizing the at least one resulting gas from the reaction mixture; c) removing excess phosphorus trichloride and also the solvent; and d) isolating 6-chlorodibenzo[d,f][1,3,2]dioxaphosphepin. |
地址 |
Essen DE |