发明名称 Process and device for polymerizing lactams molds
摘要 The invention relates to a process and device for polymerizing lactams in molds wherein the monomer, catalyst and initiator are independently fed to a mixing head feeding a mold. The system in turn comprises a series of feeding and recirculation conduits and reservoirs the temperature of which is regulated to perform the polymerization in a controlled manner.
申请公布号 US9290622(B2) 申请公布日期 2016.03.22
申请号 US201012972890 申请日期 2010.12.20
申请人 Fundacion Inasmet 发明人 García Arrieta Sonia;Palenzuela Gutierrez Luis
分类号 B29C41/42;C08G69/14;B29B7/40;B29C67/24;C08G69/16;C08G69/18;B29K77/00 主分类号 B29C41/42
代理机构 Florek & Endres PLLC 代理人 Florek & Endres PLLC
主权项 1. A method of polymerizing lactams in molds for the continuous manufacture of serial parts in corresponding molds, said manufactured parts having a variable size, geometry or composition, the method comprising: (a) continuously feeding into a mixing head a lactam, a catalyst and an initiator; wherein the lactam is at a first predetermined temperature between 70-160° C., the catalyst is at a second predetermined temperature between 20-50° C., and the initiator is at a third predetermined temperature between 20-50° C., wherein the lactam, the catalyst, and the initiator are each independently fed into the mixing head from respective independent reservoirs through respective inlets comprising valves, wherein the lactam, the catalyst and the initiator are each circulated in independent circuits at said respective first, second and third predetermined temperatures; (b) continuously mixing in the mixing head the lactam, the catalyst and the initiator, to obtain a reactive mixture; (c) continuously feeding the reactive mixture obtained in step (b) through a nozzle into a mold, wherein a volume of a casting into said mold is determined by adjusting the opening of the valves of the inlets for a time corresponding to a total volume of a polymerization mixture coming out through said nozzle, said volume of reactive mixture corresponding to a part to be manufactured, said adjustment of the opening of the valves being controlled by an automatic and programmable timer, thus allowing the automatic manufacture of serial parts having a variable size, geometry or composition; (d) allowing the reactive mixture to polymerize in the mold to obtain a molded product; and, (e) demolding the molded product.
地址 San Sebastian (Guipuzcoa) ES
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