发明名称 Shape preserving chemical transformation of ZnO mesostructures into anatase TiO<sub>2 </sub>mesostructures for optoelectronic application
摘要 The present application discloses a shape preserving chemical transformation of ZnO mesostructures into anatase TiO2 mesostructures using controlled low temperature TiCl4 treatment for optoelectronic applications.
申请公布号 US9290392(B2) 申请公布日期 2016.03.22
申请号 US201213486509 申请日期 2012.06.01
申请人 Council of Scientific & Industrial Research 发明人 Muduli Subas K.;Dhas Vivek V.;Game Onkar S.;Yengantiwar Ashish P.;Ogale Satishchandra B.
分类号 C01G23/047;C01G23/053;C01G9/02 主分类号 C01G23/047
代理机构 Blank Rome LLP 代理人 Blank Rome LLP ;Greenbaum Michael C.;Tesfazion Jamie B.
主权项 1. A process for the shape preserving chemical transformation of ZnO mesostructures into anatase TiO2 mesostructures comprising the steps of: i. treating the Zinc oxide mesostructures with Titanium tetrachloride (TiCl4) solution at temperature in the range of 60 to 70° C. for period in the range of 20 to 30 min; ii. annealing the TiCl4 treated Zinc oxide mesostructures as obtained in step (i) at a temperature in the range of 400 to 450° C. for period in the range of 20 to 30 min to obtain anatase TiO2 mesostructures.
地址 IN