发明名称 Method for supplying source gas for producing polycrystalline silicon and polycrystalline silicon
摘要 In a method according to the present invention, an occurrence ratio of popcorn is suppressed by adjusting kinetic energy of a source gas supplied to a reaction furnace for producing polycrystalline silicon with a Siemens method (flow velocity and a supply amount of the source gas in source gas supply nozzle ejection ports). Specifically, in performing deposition reaction of the polycrystalline silicon under a reaction pressure of 0.25 MPa to 0.9 MPa, when flow velocity of the source gas in gas supply ports of the source gas supply nozzles (9) is represented as u (m/sec), a source gas supply amount is represented as Q (kg/sec), and an inner volume of the reaction furnace (100) is represented as V (m3), values of u and Q of each of the source gas supply nozzles (9) are set such that a total Σ(Q×u2/V) of values Q×u2/V is equal to or larger than 2500 (kg/m·sec3).
申请公布号 US9263261(B2) 申请公布日期 2016.02.16
申请号 US201314435316 申请日期 2013.09.30
申请人 SHIN-ETSU CHEMICAL CO., LTD. 发明人 Kurosawa Yasushi;Netsu Shigeyoshi
分类号 C23C16/24;C23C16/50;C01B33/027;H01L21/02;C01B33/02;C01B33/035 主分类号 C23C16/24
代理机构 Oblon, McClelland, Maier & Neustadt, L.L.P. 代理人 Oblon, McClelland, Maier & Neustadt, L.L.P.
主权项 1. A method of supplying a source gas to a reaction furnace for producing polycrystalline silicon with a Siemens method, the method comprising: using a reaction furnace in which one or more source gas supply nozzles are disposed such that a flow pattern of the source gas in the reaction furnace is an ascending current in a reaction furnace center portion and is a descending current in a reaction furnace outer wall side portion; and setting, in performing deposition reaction of the polycrystalline silicon under a reaction pressure of 0.25 MPa to 0.9 MPa, when flow velocity of the source gas in gas supply ports of the source gas supply nozzles is represented as u (m/sec), a source gas supply amount is represented as Q (kg/sec), and an inner volume of the reaction furnace is represented as V (m3), values of u and Q of each of the source gas supply nozzles such that a total Σ(Q×u2/V) of values Q×u2/V is equal to or larger than 2500 (kg/m·sec3).
地址 Tokyo JP