发明名称 PROCESS FOR THE PRODUCTION OF ACRYLIC FIBERS
摘要 A process is described for the preparation of a homogeneous spinning solution for the production of acrylic fibers which comprises the following steps: i) preparation of a homogeneous suspension by mixing a powder homopolymer or copolymer of acrylonitrile with a mixture of DMSO/water ranging from 94.5/5.5 to 97/3% w/w at a temperature ranging from 5° C. to 10° C., preferably a mixture of DMSO/water 95/5 at a temperature of 5° C., said mixing being carried out in a time ranging from 5 to 30 minutes, by spraying a stream of the DMSO/water solvent onto a stream of powder homopolymer or copolymer of acrylonitrile, disgregated and premixed;ii) heating the homogeneous suspension coming from step i) to a temperature ranging from 70° C. to 150° C. in a time ranging of from 0.5 to 30 minutes, until the complete dissolution of the homopolymer or copolymer and the formation of a homogeneous solution. This spinning solution is then fed to a storage tank or to the spinning line.
申请公布号 US2015376391(A1) 申请公布日期 2015.12.31
申请号 US201514591330 申请日期 2015.01.07
申请人 MONTEFIBRE MAE TECHNOLOGIES S.r.l. 发明人 Francalanci Franco;Gozzo Pierluigi;Marinetti Massimo;Proserpio Roberto
分类号 C08L33/20;D01F6/18;D01F6/38;B01F5/06;B01F1/00 主分类号 C08L33/20
代理机构 代理人
主权项 1. A process for preparing a homogeneous spinning solution for the production of acrylic fibers which comprises the following steps: i) preparation of a homogeneous suspension by mixing a powder homopolymer or copolymer of acrylonitrile with a mixture of DMSO/water in an amount of from 94.5/5.5 to 97/3% w/w at a temperature of from 5° C. to 10° C., preferably a mixture of DMSO/water 95/5 at a temperature of 5° C., said mixing being carried out in a time ranging from 5 to 30 minutes, by spraying a stream of the DMSO/water solvent on a stream of powder homopolymer or copolymer of acrylonitrile, disintegrated and premixed; ii) heating the homogeneous suspension coming from step i) at a temperature ranging from 70° C. to 150° C. in a time ranging of from 0.5 to 30 minutes, until the complete dissolution of the homopolymer or copolymer and the formation of a homogeneous solution.
地址 Milano IT