发明名称 Mesoporous Zinc Oxide Powder and Method for Production Thereof
摘要 A method of manufacturing a zinc oxide powder including synthesizing a mesoporous zinc oxide precursor powder by adding an aqueous solution of zinc chloride to an aqueous solution of sodium carbonate while agitating to cause precipitation of a mesoporous zinc carbonate powder wherein the molar ratio of zinc chloride to sodium carbonate present when the aqueous solution of zinc chloride and the aqueous solution of sodium carbonate are reacted is at least 1:2, heat treating a mesoporous zinc precursor material to form the mesoporous zinc oxide powder at a heat treatment temperature in the range of 250-575° C. The zinc oxide powder includes mesoporous zinc oxide aggregates with a plurality of primary zinc oxide crystallites bonded together at shared interfaces.
申请公布号 US2015376025(A1) 申请公布日期 2015.12.31
申请号 US201514850281 申请日期 2015.09.10
申请人 Antaria Limited 发明人 McCormick Paul;Trotter Geoffrey
分类号 C01G9/02 主分类号 C01G9/02
代理机构 代理人
主权项 1. A method of manufacturing a zinc oxide powder comprising: synthesizing a mesoporous zinc oxide precursor powder by adding an aqueous solution of zinc chloride to an aqueous solution of sodium carbonate whilst agitating to cause precipitation of a mesoporous zinc carbonate powder wherein the molar ratio of zinc chloride to sodium carbonate present when the aqueous solution of zinc chloride and the aqueous solution of sodium carbonate are reacted is at least 1:2; and, heat treating a mesoporous zinc precursor material to form the mesoporous zinc oxide powder at a heat treatment temperature in the range of 250-575° C., and, wherein the zinc oxide powder comprises mesoporous zinc oxide aggregates comprising a plurality of primary zinc oxide crystallites bonded together at shared interfaces, the aggregates having a number average aggregate size of at least 0.8 micron, wherein the aggregates have a total mesopore volume of at least 0.5 cm3/g, a pore size in the range of 2 nm to 100 nm, and, a surface area in the range of 20 to 70 m2/g.
地址 Bentley AU