发明名称 |
FACILE METHOD FOR PREPARATION OF 5-NITROTETRAZOLATES USING A BATCH SYSTEM |
摘要 |
Described are methods for preparing salts of 5-nitrotetrazolate by reacting 5-aminotetrazole, an acid, and sodium nitrite in water in a batch reaction at an elevated temperature. As examples, the acid is nitric acid, sulfuric acid, perchloric acid, or hydrochloric acid, and the elevated temperature is at or above 65° C. |
申请公布号 |
US2015361057(A1) |
申请公布日期 |
2015.12.17 |
申请号 |
US201514731613 |
申请日期 |
2015.06.05 |
申请人 |
SRI International ;Pacific Scientific Energetic Materials Company |
发明人 |
Bottaro Jeffrey C.;Petrie Mark A.;Bragg Jon G.;Fronabarger John W.;Williams Michael D. |
分类号 |
C07D257/06 |
主分类号 |
C07D257/06 |
代理机构 |
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代理人 |
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主权项 |
1. A method of preparing salts of 5-nitrotetrazolate comprising reacting 5-aminotetrazole, an acid, and sodium nitrite in water in a batch reaction at an elevated temperature. |
地址 |
Menlo Park CA US |