发明名称 Metal powder production method, metal powder produced thereby, conductive paste and multilayer ceramic electronic component
摘要 Fine, highly-crystallized metal powder is produced at low cost and high efficiency by a method involving: ejecting raw material powder composed of one or more kinds of thermally decomposable metal compound powders into a reaction vessel through a nozzle together with a carrier gas and producing a metal powder by heating the raw material powder at a temperature T2 which is higher than the decomposition temperature of the raw material powder and not lower than (Tm−200°) C. where Tm is the melting point (° C.) of the metal to be produced, while allowing the raw material powder to pass through the reaction vessel in a state where the raw material powder is dispersed in a gas phase at a concentration of 10 g/liter or less, wherein an ambient temperature T1 of a nozzle opening part is set to a temperature of 400° C. or higher and lower than (Tm−200°) C.
申请公布号 US9162288(B2) 申请公布日期 2015.10.20
申请号 US201213600317 申请日期 2012.08.31
申请人 SHOEI CHEMICAL INC. 发明人 Akimoto Yuji;Nagashima Kazuro;Ieda Hidenori;Maekawa Masayuki
分类号 B22F9/30;H01B1/22;B22F1/00 主分类号 B22F9/30
代理机构 Flynn, Thiel, Boutell & Tanis, P.C. 代理人 Flynn, Thiel, Boutell & Tanis, P.C.
主权项 1. A method for producing a crystallized metal powder, the method comprising: ejecting a raw material powder composed of one or more kinds of thermally decomposable metal compound powders into a reaction vessel through a nozzle together with a carrier gas under the condition of V/S >600, where V represents a flow rate per unit time of the carrier gas (liter/min) and S represents a cross-sectional area of a nozzle opening part (cm2); and producing a metal powder by heating the raw material powder at a temperature T2 which is higher than a decomposition temperature of the raw material powder and not lower than (Tm−200°) C. where Tm is the melting point (° C.) of the metal to be produced, while allowing the raw material powder to pass through the reaction vessel in a state where the raw material powder is dispersed in a gas phase at a concentration of 10 g/liter or less, wherein an ambient temperature T1 of the nozzle opening part is set to a temperature which is higher than the decomposition temperature of the raw material powder and is at least 400° C. and lower than (Tm−200°) C. and the raw material powder is exposed to the temperature T1 immediately after being ejected into the reaction vessel wherein the temperature T1 causes the raw material powder to undergo pyrolysis and generate a pyrolysis gas.
地址 Shinjuku-ku, Tokyo JP