发明名称 PURIFICATION METHOD FOR 2-METHYLNAPHTHALENE
摘要 PURPOSE:To recover the titled high-purity compound without containing impurities, e.g. organic sulfur, organic nitrogen compounds, etc., in high yield, by adding and dissolving a hydroxylamine derivative in crude 2-methylnaphthalene, cooling the resultant solution and separating deposited crystal substance. CONSTITUTION:A hydroxylamine derivative, particularly preferably mono ethanolamine, diethanolamine, triethanolamine, propanolamine or butanolamine is added to crude 2-methylnaphthalene, particularly preferably crude 2- methylnaphthalene containing >=90wt.%, more preferably 95-97wt.% 2- methylnaphthalene to selectively extract and remove impurities organic sulfur compounds or organic nitrogen compounds and the deposited crystal substance 2-methylnaphthalene is recovered. The amount of the added hydroxylamine derivative, particularly monoethanolamine used is 2-4 times based on the 2- methylnaphthalene.
申请公布号 JPS63122637(A) 申请公布日期 1988.05.26
申请号 JP19860268903 申请日期 1986.11.11
申请人 SUMIKIN CHEM CO LTD 发明人 TAKEYA SHOJI;NAKAMURA TAKENORI
分类号 C07C7/14;C07C1/00;C07C15/24;C07C67/00 主分类号 C07C7/14
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